Mass: 18.015 Da / Num. of mol.: 171 / Source method: isolated from a natural source / Formula: H2O
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 1.98 Å3/Da / Density % sol: 38.1 %
Crystal grow
Method: vapor diffusion, sitting drop / pH: 4.5 Details: CHICKEN EGG WHITE LYSOZYME (FLUKA) HAS BEEN DISSOLVED IN 50 MM SODIUM ACETATE BUFFER PH 4.57 AND CRYSTALLIZED BY SITTING DROP DIFFUSION METHOD. EACH DROP CONTAINED 20 MG/ML OF LYSOZYME AND 5. ...Details: CHICKEN EGG WHITE LYSOZYME (FLUKA) HAS BEEN DISSOLVED IN 50 MM SODIUM ACETATE BUFFER PH 4.57 AND CRYSTALLIZED BY SITTING DROP DIFFUSION METHOD. EACH DROP CONTAINED 20 MG/ML OF LYSOZYME AND 5.5 PERCENT OF NACL IN 25 MM OF NA[AC] PH 4.57
Resolution: 1.5→39.17 Å / Cor.coef. Fo:Fc: 0.967 / Cor.coef. Fo:Fc free: 0.932 / SU B: 1.384 / SU ML: 0.052 / Cross valid method: THROUGHOUT / ESU R: 0.079 / ESU R Free: 0.084 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.21094
947
5 %
RANDOM
Rwork
0.16755
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obs
0.16971
17978
100 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.4 Å / Solvent model: MASK