#1: ジャーナル: Protein Pept.Lett. / 年: 2007 タイトル: Crystallization and Preliminary Diffraction Studies of Porcine Pancreatic Elastase in Complex with a Novel Inhibitor 著者: Oliveira, T.F. / Mulchande, J. / Moreira, R. / Iley, J. / Archer, M.
SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AB" IN EACH CHAIN ON SHEET RECORDS BELOW ... SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AB" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 6-STRANDED BARREL THIS IS REPRESENTED BY A 7-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL.
THIS SEQUENCE BELONGS TO THE PRECURSOR OF PORCINE PANCREATIC ELASTASE. FOR THE CRYSTALLOGRAPHIC ...THIS SEQUENCE BELONGS TO THE PRECURSOR OF PORCINE PANCREATIC ELASTASE. FOR THE CRYSTALLOGRAPHIC STUDIES HAVE BEEN USED THE AMINO-ACID SEQUENCE FROM 27 TO 266
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 2.1 Å3/Da / 溶媒含有率: 41 % / 解説: NONE
結晶化
pH: 5.1 / 詳細: 100 MM SODIUM ACETATE PH 5.1 200 MM SODIUM SULFATE
解像度: 1.67→33.84 Å / Cor.coef. Fo:Fc: 0.962 / Cor.coef. Fo:Fc free: 0.941 / SU B: 1.487 / SU ML: 0.052 / 交差検証法: THROUGHOUT / ESU R: 0.1 / ESU R Free: 0.095 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
反射数
%反射
Selection details
Rfree
0.186
1310
5.1 %
RANDOM
Rwork
0.156
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obs
0.158
24355
98.5 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK