Text: NOE DATA FROM EXPERIMENTS ON 13C,15N-LABELED SAMPLE. STRUCTURES REFINED USING 209 RESIDUAL 1H-15N DIPOLAR COUPLING RESTRAINTS FROM MEASUREMENTS MADE IN TWO DIFFERENT LIQUID CRYSTALLINE PHASES.
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試料調製
試料状態
pH: 3.8 / 圧: 1 atm / 温度: 308 K
結晶化
*PLUS
手法: other / 詳細: NMR
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NMR測定
NMRスペクトロメーター
タイプ
製造業者
モデル
磁場強度 (MHz)
Spectrometer-ID
Home-built home built
Home-built
homebuilt
500
1
Home-built home built
Home-built
homebuilt
600
2
Bruker DMX
Bruker
DMX
750
3
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解析
NMR software
名称
開発者
分類
X-PLOR
BRUNGER
精密化
X-PLOR
構造決定
精密化
手法: simulated annealing / ソフトェア番号: 1 詳細: DETAILS OF THE NMR DATA USED IN THE STRUCTURE CALCULATIONS ARE AS FOLLOWS NUMBER OF RESTRAINTS NOE DISTANCE RESTRAINTS 1632 HYDROGEN BOND RESTRAINTS 60 DIHEDRAL ANGLE PHI RESTRAINTS 51 ...詳細: DETAILS OF THE NMR DATA USED IN THE STRUCTURE CALCULATIONS ARE AS FOLLOWS NUMBER OF RESTRAINTS NOE DISTANCE RESTRAINTS 1632 HYDROGEN BOND RESTRAINTS 60 DIHEDRAL ANGLE PHI RESTRAINTS 51 DIHEDRAL ANGLE CHI 1 RESTRAINTS 59 RESIDUAL DIPOLAR COUPLING RESTRAINTS 209 RMS DEVIATIONS FROM EXPERIMENTAL RESTRAINTS NOE RESTRAINTS (ANGSTROMS) 0.0439 DIHEDRAL RESTRAINTS (DEGREES) 0.655 DIPOLAR COUPLING RESTRAINTS (HZ) 1.159 RMS DEVIATIONS FROM IDEAL COVALENT GEOMETRY BONDS (ANGSTROMS) 0.00333 ANGLES (DEGREES) 0.492 IMPROPERS (DEGREES) 0.384
NMRアンサンブル
コンフォーマー選択の基準: LOWEST ENERGY / 計算したコンフォーマーの数: 300 / 登録したコンフォーマーの数: 50