8ENT
Interleukin-21 signaling complex with IL-21R and IL-2Rg
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-02-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 |
Unit cell lengths | 66.167, 66.464, 162.684 |
Unit cell angles | 83.34, 83.71, 73.10 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.170 | 2.932 |
High resolution limit [Å] | 2.830 | 2.831 |
Rpim | 0.129 | |
Number of reflections | 57754 | 5757 |
<I/σ(I)> | 4.22 | |
Completeness [%] | 91.7 | |
Redundancy | 3.7 | |
CC(1/2) | 0.985 | 0.401 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 295 | 0.1M Tris pH 8, 20% PEG 6000 |