6SS6
Structure of arginase-2 in complex with the inhibitory human antigen-binding fragment Fab C0020187
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.91587 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 138.126, 138.126, 551.307 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.780 | 3.360 |
High resolution limit [Å] | 3.250 | 3.250 |
Rmerge | 0.780 | 8.480 |
Number of reflections | 50453 | 4555 |
<I/σ(I)> | 4.2 | 0.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 10.4 | 9.9 |
CC(1/2) | 0.990 | 0.500 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 2 M (NH4)2SO4 |