4U7P
Crystal structure of DNMT3A-DNMT3L complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-11-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.2816 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 252.031, 252.031, 75.336 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.960 |
High resolution limit [Å] | 3.820 | 8.220 | 3.820 |
Rmerge | 0.098 | 0.044 | 0.870 |
Rmeas | 0.108 | 0.049 | 0.958 |
Rpim | 0.046 | 0.021 | 0.397 |
Total number of observations | 80080 | ||
Number of reflections | 14153 | ||
<I/σ(I)> | 6.9 | ||
Completeness [%] | 99.9 | 99.2 | 99.9 |
Redundancy | 5.7 | 5.2 | 5.8 |
CC(1/2) | 0.996 | 0.688 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.6 | 291 | 0.05M Bis-Tris, 0.1M Sodium Malonate, 8% PEG3350 |