2X6V
Crystal structure of human TBX5 in the DNA-bound and DNA-free form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 118.240, 118.240, 243.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.707 - 2.200 |
R-factor | 0.1986 |
Rwork | 0.197 |
R-free | 0.22520 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1h6f |
RMSD bond length | 0.009 |
RMSD bond angle | 1.261 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.070 | 0.430 |
Number of reflections | 51044 | |
<I/σ(I)> | 11 | 2.8 |
Completeness [%] | 98.7 | 97 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6 | 0.1 M MES PH 5.6, 0.2 M MGCL2, 0.2 M NACL, 5% PEG 6K |