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2P4S

Structure of Purine Nucleoside Phosphorylase from Anopheles gambiae in complex with DADMe-ImmH

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X29A
Synchrotron siteNSLS
BeamlineX29A
Temperature [K]100
Detector technologyCCD
Collection date2006-09-11
DetectorADSC QUANTUM 315
Wavelength(s)0.97910
Spacegroup nameP 41 21 2
Unit cell lengths106.718, 106.718, 240.388
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution8.000 - 2.200
R-factor0.17726
Rwork0.175
R-free0.21667
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1rr6
RMSD bond length0.020
RMSD bond angle1.722
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareREFMAC
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.280
High resolution limit [Å]2.2002.200
Rmerge0.1220.321
Number of reflections66744
<I/σ(I)>5.52.1
Completeness [%]93.159.6
Redundancy356.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP4.62980.1 M Sodium Acetate, 4.0 M Ammonium Acetate, pH 4.6, VAPOR DIFFUSION, SITTING DROP, temperature 298K

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