8W7C
Activation of mitochondrial Caseinolytic Protease P (ClpP) induces selective cancer cell lethality
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-06-12 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 142.245, 153.591, 104.617 |
Unit cell angles | 90.00, 117.96, 90.00 |
Refinement procedure
Resolution | 46.200 - 3.000 |
R-factor | 0.2407 |
Rwork | 0.240 |
R-free | 0.25990 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.880 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.18.2_3874: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 97.344 | 3.070 |
High resolution limit [Å] | 2.920 | 2.920 |
Number of reflections | 77808 | 41644 |
<I/σ(I)> | 6.3 | |
Completeness [%] | 96.1 | |
Redundancy | 3.7 | |
CC(1/2) | 0.982 | 0.982 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 289 | 200 mM KCl, 100 mM MES, 12%PEG4000 |