Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 5.0.2 |
| Synchrotron site | ALS |
| Beamline | 5.0.2 |
| Temperature [K] | 95 |
| Detector technology | CCD |
| Collection date | 2015-06-28 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 107.060, 107.060, 243.490 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 20.000 - 4.400 |
| Rwork | 0.318 |
| R-free | 0.34100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | CNS |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 49.370 | 49.380 | 4.490 |
| High resolution limit [Å] | 4.340 | 9.330 | 4.340 |
| Rmerge | 0.061 | 0.021 | 0.313 |
| Rmeas | 0.069 | 0.024 | 0.353 |
| Rpim | 0.031 | 0.011 | 0.160 |
| Number of reflections | 5518 | 680 | 123 |
| <I/σ(I)> | 17.5 | 56.6 | 4.7 |
| Completeness [%] | 90.8 | 97.7 | 21.21 |
| Redundancy | 5.01 | 4.35 | 4.46 |
| CC(1/2) | 0.999 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 294.15 | 30% 2-methyl-2,4 pentanediol (MPD), 0.1 M sodium citrate pH 5.6 - 6.5 |
