8GTJ
Crystal structure of IpaH7.8-LRR and GSDMB isoform-4 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2021-09-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97852 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 88.338, 88.338, 335.624 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.770 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.097 | 0.853 |
Rmeas | 0.100 | 0.875 |
Number of reflections | 42928 | 3147 |
<I/σ(I)> | 26.13 | 3.34 |
Completeness [%] | 99.9 | 100 |
Redundancy | 18.4 | 19.6 |
CC(1/2) | 0.999 | 0.894 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.2 | 293 | 1.2 M Sodium potassium phosphate |