7ZKX
SRPK2 IN COMPLEX WITH INHIBITOR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-01-16 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.99989 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 107.755, 107.755, 90.228 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 93.320 - 2.060 |
R-factor | 0.1807 |
Rwork | 0.179 |
R-free | 0.20750 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2x7g |
RMSD bond length | 0.011 |
RMSD bond angle | 1.536 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 93.320 | 2.310 |
High resolution limit [Å] | 2.060 | 2.060 |
Rmeas | 0.050 | 0.584 |
Number of reflections | 36972 | 10714 |
<I/σ(I)> | 15.51 | 2.53 |
Completeness [%] | 97.9 | 98.8 |
Redundancy | 2.9 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 5 mM HEPES pH 7.5, 150 mM NaCl, 20 mM DTT |