7KX0
Crystal structure of the CD27:CD70 co-stimulatory complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 109.530, 113.630, 163.510 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 93.310 | 2.980 |
High resolution limit [Å] | 2.690 | 2.690 |
Rmerge | 0.105 | 1.180 |
Rpim | 0.044 | 0.479 |
Number of reflections | 18602 | 931 |
<I/σ(I)> | 12 | 1.7 |
Completeness [%] | 64.9 | 12.4 |
Redundancy | 6.7 | 7 |
CC(1/2) | 0.998 | 0.727 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 291 | 100 mM Tris hydrochloride pH 8 40 % 2-methyl-2,4-pentanediol |