7B0I
Structure of a minimal SF3B core in complex with spliceostatin A (form II)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 108.503, 108.503, 358.938 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.410 | 3.040 |
High resolution limit [Å] | 2.950 | 2.950 |
Rmerge | 0.116 | 6.113 |
Rmeas | 0.119 | 6.275 |
Rpim | 0.027 | 1.403 |
Number of reflections | 52617 | 4460 |
<I/σ(I)> | 17.6 | 0.6 |
Completeness [%] | 99.9 | 99.7 |
Redundancy | 19.8 | 19.6 |
CC(1/2) | 1.000 | 0.402 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.17 | 277.15 | 0.1 M HEPES pH=7.17, 0.2 M MgCl2, 25% (v/v) PEG-400 |