7AHV
Anti-FIXa Fab of mim8 in complex with human FIXa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-14 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 41 2 2 |
Unit cell lengths | 97.030, 97.030, 254.510 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.520 | 3.216 |
High resolution limit [Å] | 3.105 | 3.105 |
Rmerge | 0.692 | 2.568 |
Rmeas | 0.721 | 2.672 |
Rpim | 0.199 | 0.730 |
Number of reflections | 22811 | 28675 |
<I/σ(I)> | 4.3 | 0.95 |
Completeness [%] | 99.8 | 99.19 |
Redundancy | 13 | 13 |
CC(1/2) | 0.957 | 0.476 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 291 | 2 M ammonium sulphate, 0.1 M Hepes, pH 7.5 |