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6ZG9

Structure of M1-StaR-T4L in complex with GSK1034702 at 2.5A

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I24
Synchrotron siteDiamond
BeamlineI24
Temperature [K]100
Detector technologyPIXEL
Collection date2012-07-27
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.96860
Spacegroup nameP 21 21 21
Unit cell lengths62.363, 66.571, 153.102
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution33.970 - 2.500
R-factor0.205
Rwork0.203
R-free0.24200
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2y00
RMSD bond length0.009
RMSD bond angle0.950
Data reduction softwareMOSFLM
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwareBUSTER (2.11.7)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]76.5512.627
High resolution limit [Å]2.5002.500
Rpim0.1981.857
Number of reflections14062506
<I/σ(I)>4.8
Completeness [%]91.2
Redundancy8.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1LIPIDIC CUBIC PHASE2930.1 NaHEPES pH 7.4-7.8, 0.1M di-ammonium hydrogenohosphate, 30-38% PEG300

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