6Y54
Crystal structure of a Neisseria meningitidis serogroup A capsular oligosaccharide bound to a functional Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 52.609, 153.205, 101.051 |
Unit cell angles | 90.00, 91.53, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.740 | 2.760 |
High resolution limit [Å] | 2.670 | 2.670 |
Number of reflections | 44254 | 4231 |
<I/σ(I)> | 6.4 | |
Completeness [%] | 97.6 | |
Redundancy | 3.1 | |
CC(1/2) | 0.979 | 0.598 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 100 mM MES pH 5.4, 255 mM KI 25% PEG 4000 |