6WJC
Muscarinic acetylcholine receptor 1 - muscarinic toxin 7 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-13 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.033 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 122.148, 150.429, 76.927 |
Unit cell angles | 90.00, 98.77, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.310 | 46.310 | 2.650 |
High resolution limit [Å] | 2.550 | 9.540 | 2.550 |
Rmerge | 0.040 | 0.020 | 1.093 |
Rmeas | 0.048 | 0.024 | 1.291 |
Rpim | 0.026 | 0.013 | 0.682 |
Total number of observations | 149894 | 2639 | 16394 |
Number of reflections | 44412 | 823 | 4664 |
<I/σ(I)> | 12.4 | 35.8 | 1.2 |
Completeness [%] | 99.4 | 94 | 99.9 |
Redundancy | 3.4 | 3.2 | 3.5 |
CC(1/2) | 0.999 | 0.999 | 0.649 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 22-27% SOKALAN, HEPES(7.5), 0.1M NaCl |