Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

6ULA

Crystal structure of human GAC in complex with inhibitor UPGL00012

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCHESS BEAMLINE A1
Synchrotron siteCHESS
BeamlineA1
Temperature [K]100
Detector technologyCCD
Collection date2015-05-29
DetectorADSC QUANTUM 210
Wavelength(s)0.98
Spacegroup nameP 1 21 1
Unit cell lengths98.723, 138.888, 177.154
Unit cell angles90.00, 89.98, 90.00
Refinement procedure
Resolution37.890 - 2.950
R-factor0.2177
Rwork0.217
R-free0.27920
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)5d3o
RMSD bond length0.011
RMSD bond angle1.488
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHENIX
Refinement softwarePHENIX (1.15.2_3472)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.750
High resolution limit [Å]2.7002.700
Rmeas0.185
Number of reflections1247376102
<I/σ(I)>9.14
Completeness [%]97.295.7
Redundancy3.33.1
CC(1/2)0.528
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP829312% PEG6000, 1.0M LiCl, pH 8.0

227111

PDB entries from 2024-11-06

PDB statisticsPDBj update infoContact PDBjnumon