Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
| Synchrotron site | PETRA III, EMBL c/o DESY |
| Beamline | P14 (MX2) |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-10-01 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.976 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 634.870, 121.980, 264.420 |
| Unit cell angles | 90.00, 112.91, 90.00 |
Refinement procedure
| Resolution | 48.764 - 6.000 |
| R-factor | 0.2345 |
| Rwork | 0.234 |
| R-free | 0.27210 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2win |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.565 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.760 | 6.270 |
| High resolution limit [Å] | 6.000 | 6.000 |
| Number of reflections | 47262 | 5785 |
| <I/σ(I)> | 5.17 | |
| Completeness [%] | 99.5 | 99.9 |
| Redundancy | 6.249 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 277 | 50 mM MgAcetate 50 mM Mes 6.5 5 % w/v PEG 10K |
