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6NN8

The structure of human liver pyruvate kinase, hLPYK-S531E

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL9-2
Synchrotron siteSSRL
BeamlineBL9-2
Temperature [K]100
Detector technologyPIXEL
Collection date2018-12-10
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.97946
Spacegroup nameP 1 21 1
Unit cell lengths94.909, 139.410, 181.286
Unit cell angles90.00, 103.35, 90.00
Refinement procedure
Resolution39.538 - 2.416
R-factor0.2085
Rwork0.208
R-free0.26010
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4ip7
RMSD bond length0.013
RMSD bond angle1.318
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwarePHENIX ((1.13_2998: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]39.5382.460
High resolution limit [Å]2.4162.416
Number of reflections173222
<I/σ(I)>16.4
Completeness [%]98.9
Redundancy7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP2980.2 M ammonium citrate, pH 5.6, 16% PEG3350

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