6NFM
Crystal Structure of the Cancer Genomic DNA Mutator APOBEC3B with loop 7 from APOBEC3G
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-26 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.979 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 50.314, 50.314, 149.808 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.766 - 2.530 |
R-factor | 0.2207 |
Rwork | 0.218 |
R-free | 0.27570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5cqd |
RMSD bond length | 0.003 |
RMSD bond angle | 0.531 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_3357: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.800 | 2.620 |
High resolution limit [Å] | 2.530 | 2.530 |
Rmerge | 0.180 | 1.900 |
Rmeas | 0.190 | 1.900 |
Rpim | 0.070 | 0.700 |
Number of reflections | 6968 | 674 |
<I/σ(I)> | 10.9 | 1.2 |
Completeness [%] | 99.9 | 100 |
Redundancy | 7.5 | 7.8 |
CC(1/2) | 0.996 | 0.500 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | LiCl, HEPES,PEG3350 |