6L71
Sirtuin 2 demyristoylation native intermediate I & II mixture
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-03-23 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97930 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 37.601, 78.095, 56.347 |
Unit cell angles | 90.00, 97.64, 90.00 |
Refinement procedure
Resolution | 27.924 - 2.109 |
R-factor | 0.1704 |
Rwork | 0.167 |
R-free | 0.22350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4r8m |
RMSD bond length | 0.009 |
RMSD bond angle | 1.216 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.150 |
High resolution limit [Å] | 2.109 | 2.109 |
Number of reflections | 18062 | 712 |
<I/σ(I)> | 11 | 1.5 |
Completeness [%] | 96.7 | |
Redundancy | 5.9 | |
CC(1/2) | 0.989 | 0.601 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 291 | 0.1M MES, pH 6.5, 6%-20% (w/v) PEG 10000 |