6JTZ
Crystal Structure of hRecQ1_D2-Zn-WH containing mutation on beta-hairpin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2018-11-28 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 52.950, 101.835, 73.434 |
Unit cell angles | 90.00, 99.07, 90.00 |
Refinement procedure
Resolution | 19.690 - 2.797 |
R-factor | 0.2293 |
Rwork | 0.227 |
R-free | 0.28170 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v1x |
Data reduction software | XDS |
Data scaling software | SCALA (3.3.22) |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 72.516 | 19.690 | 2.950 |
High resolution limit [Å] | 2.797 | 8.850 | 2.800 |
Rmerge | 0.031 | 0.366 | |
Rmeas | 0.100 | 0.036 | 0.426 |
Rpim | 0.051 | 0.019 | 0.217 |
Number of reflections | 18892 | 567 | 2709 |
<I/σ(I)> | 12.2 | 19.7 | 2.1 |
Completeness [%] | 99.0 | 90.6 | 98 |
Redundancy | 3.8 | 3.6 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 65% v/v Tacsimate pH=7.0 |