6H8K
Crystal structure of a variant (Q133C in PSST) of Yarrowia lipolytica complex I
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-26 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0000 |
Spacegroup name | H 3 2 |
Unit cell lengths | 316.310, 316.310, 819.180 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.000 - 3.790 |
R-factor | 0.361 |
Rwork | 0.361 |
R-free | 0.36300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wz7 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.230 |
Data reduction software | XDS |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.990 |
High resolution limit [Å] | 3.790 | 3.790 |
Rmerge | 0.204 | |
Number of reflections | 120019 | |
<I/σ(I)> | 13.2 | 0.7 |
Completeness [%] | 99.6 | |
Redundancy | 21 | |
CC(1/2) | 1.000 | 0.439 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 291 | PEG 3350, calcium acetate, glycerol |