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6F8X

Crystal structure of the PDE4D catalytic domain in complex with GEBR-26g

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06DA
Synchrotron siteSLS
BeamlineX06DA
Temperature [K]100
Detector technologyPIXEL
Collection date2016-08-20
DetectorPSI PILATUS 6M
Wavelength(s)1
Spacegroup nameP 21 21 21
Unit cell lengths98.547, 119.820, 64.502
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution49.208 - 1.950
R-factor0.1684
Rwork0.167
R-free0.20460
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)6f6u
RMSD bond length0.007
RMSD bond angle0.932
Data reduction softwareXDS
Phasing softwarePHENIX
Refinement softwarePHENIX (1.9_1692)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]49.2082.266
High resolution limit [Å]1.9501.950
Rmerge0.124
Number of reflections107507
<I/σ(I)>13
Completeness [%]100.0
Redundancy13
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP293Hepes PEG 3350 Magnesium Chloride

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