6DC8
Fab/epitope complex of mouse monoclonal antibody 8B2 targeting a non-phosphorylated tau epitope.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL14-1 |
Synchrotron site | SSRL |
Beamline | BL14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-10-09 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.979 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 68.836, 68.836, 198.853 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.302 - 1.799 |
R-factor | 0.1811 |
Rwork | 0.179 |
R-free | 0.21870 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.912 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.300 | 1.860 |
High resolution limit [Å] | 1.790 | 1.790 |
Number of reflections | 45390 | |
<I/σ(I)> | 14.5 | |
Completeness [%] | 99.9 | |
Redundancy | 1.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 23% polyethylene glycol 8000, 0.17 M ammonium acetate, and 0.085 M sodium cacodylate trihydrate pH 6.5 |