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6C19

FGFR1 kinase complex with inhibitor SN36985

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007 HF
Temperature [K]110
Detector technologyIMAGE PLATE
Collection date2015-01-20
DetectorMAR scanner 345 mm plate
Wavelength(s)1.5418
Spacegroup nameC 1 2 1
Unit cell lengths208.426, 49.013, 64.628
Unit cell angles90.00, 105.97, 90.00
Refinement procedure
Resolution19.710 - 2.120
R-factor0.20704
Rwork0.205
R-free0.23852
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4wun
RMSD bond length0.011
RMSD bond angle1.588
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0049)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]19.7102.180
High resolution limit [Å]2.1202.120
Rmerge0.0800.682
Rpim0.0340.293
Number of reflections213152944
<I/σ(I)>19.93.1
Completeness [%]99.9100
Redundancy7.47.2
CC(1/2)0.9990.854
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP29120% MPEG 5000, 0.1 M sodium cacodylate pH 7.5, 0.2 M ammonium sulfate

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