6BSX
CRYSTAL STRUCTURE OF RHEB IN COMPLEX WITH COMPOUND 1 AT 1.65A RESOLUTION
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-12-05 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.9787 |
Spacegroup name | P 1 |
Unit cell lengths | 49.370, 49.720, 70.970 |
Unit cell angles | 89.99, 77.70, 89.87 |
Refinement procedure
Resolution | 29.264 - 1.650 |
R-factor | 0.1986 |
Rwork | 0.197 |
R-free | 0.24380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1xtq |
RMSD bond length | 0.016 |
RMSD bond angle | 1.508 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX (DEV_1883) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.690 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.049 | 0.319 |
Number of reflections | 73559 | |
<I/σ(I)> | 10.09 | 2.5 |
Completeness [%] | 92.7 | 93.4 |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 8.8 | 293 | 28% PEG4000, 0.2M SODIUM ACETATE, 0.1M TRIS-HCL, PH 8.8, SITTING DROP, TEMPERATURE 293K |