6BRR
Crystal structure of DNMT3A (R836A)-DNMT3L in complex with DNA containing two CpG sites
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-06-26 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.98 |
Spacegroup name | H 3 |
Unit cell lengths | 205.005, 205.005, 89.358 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.955 - 2.970 |
R-factor | 0.2017 |
Rwork | 0.199 |
R-free | 0.24160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qrv |
RMSD bond length | 0.004 |
RMSD bond angle | 0.665 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 3.060 |
High resolution limit [Å] | 2.970 | 2.970 |
Rmerge | 0.065 | 1.205 |
Number of reflections | 28270 | |
<I/σ(I)> | 13.3 | |
Completeness [%] | 98.0 | |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1 M Tris-HCl (pH 7.0), 200 mM NaH2PO4 and 5% PEG4000 |