6WVW
Crystal structure of the R59P-SNAP25 containing SNARE complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-12-08 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97946 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 48.761, 45.899, 109.066 |
Unit cell angles | 90.00, 94.41, 90.00 |
Refinement procedure
Resolution | 42.290 - 2.110 |
Rwork | 0.200 |
R-free | 0.24400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1n7s |
RMSD bond length | 0.005 |
RMSD bond angle | 0.680 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.18) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.290 | 2.186 |
High resolution limit [Å] | 2.110 | 2.110 |
Rmerge | 0.155 | |
Number of reflections | 19820 | 498 |
<I/σ(I)> | 11.2 | |
Completeness [%] | 89.6 | |
Redundancy | 11.4 | |
CC(1/2) | 0.999 | 0.374 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | 100 mM MES (pH 6.0), 100 mM CaCl2, 20-25% (v/v) |