6I5N

Crystal structure of SOCS2:Elongin C:Elongin B in complex with growth hormone receptor peptide

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-09-24
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	0.9795
Spacegroup name	P 21 21 2
Unit cell lengths	113.177, 156.763, 57.571
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	54.042 - 1.980
R-factor	0.1909
Rwork	0.190
R-free	0.22640
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.064
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((dev_2420: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	113.550	2.010
High resolution limit [Å]	1.980	1.980
Rmerge	0.094
Number of reflections	73251
<I/σ(I)>	17.1
Completeness [%]	100.0
Redundancy	13.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277.15	Sodium cacodylate, cobalt chloride, MES, ammonium sulphate