6BRW
JAK2 JH2 in complex with XMU-MP-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-12-18 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 44.386, 57.147, 60.398 |
Unit cell angles | 90.00, 110.24, 90.00 |
Refinement procedure
Resolution | 41.646 - 2.031 |
R-factor | 0.1968 |
Rwork | 0.194 |
R-free | 0.24960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4fvp |
RMSD bond length | 0.005 |
RMSD bond angle | 0.808 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.700 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmeas | 0.226 | 0.175 |
Number of reflections | 18266 | |
<I/σ(I)> | 8.3 | |
Completeness [%] | 97.5 | |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 277 | 0.1M Tris, pH 8.0 0.2M Sodium acetate 12-20% PEG 4,000 |