5ZOF
Crystal Structure of D181A/R192F hFen1 in complex with DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2016-12-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.00 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 47.670, 92.730, 102.780 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.820 - 2.249 |
R-factor | 0.237 |
Rwork | 0.235 |
R-free | 0.26880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3q8k |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 27.820 | 27.820 | 2.310 |
High resolution limit [Å] | 2.240 | 10.060 | 2.250 |
Rmerge | 0.091 | 0.069 | 0.579 |
Rmeas | 0.101 | 0.077 | 0.673 |
Number of reflections | 22092 | 263 | 1535 |
<I/σ(I)> | 11.12 | 19.18 | 2.15 |
Completeness [%] | 98.8 | 87.4 | 93.1 |
Redundancy | 5.74 | 4.859 | 3.762 |
CC(1/2) | 0.994 | 0.990 | 0.738 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.8 | 298 | PEG 3350, MgCl2, Tris, KCl |