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5ZK5

Stapled-peptides tailored against initiation of translation

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID29
Synchrotron siteESRF
BeamlineID29
Temperature [K]100
Detector technologyPIXEL
Collection date2017-06-27
DetectorDECTRIS PILATUS 6M-F
Wavelength(s)0.983998
Spacegroup nameP 21 21 21
Unit cell lengths37.480, 65.090, 76.390
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 2.250
R-factor0.20176
Rwork0.198
R-free0.26839
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4tpw
RMSD bond length0.009
RMSD bond angle1.748
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0189)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.680
High resolution limit [Å]1.5901.590
Number of reflections93191457
<I/σ(I)>16.113.13
Completeness [%]99.4
Redundancy8.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.529530%(w/v) PEG6000, 0.1M Na-Hepes pH 6.5

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