5X6V
Crystal structure of human heteroheptameric complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-10-13 |
Detector | MAR scanner 300 mm plate |
Wavelength(s) | 0.90000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.099, 93.476, 125.452 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 125.450 | 2.060 |
High resolution limit [Å] | 2.020 | 2.020 |
Number of reflections | 57406 | |
<I/σ(I)> | 13.6 | |
Completeness [%] | 99.4 | |
Redundancy | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | sodium citrate, ammonium acetate, PEG 4000 |