5W0R
Crystal structure of MBP fused activation-induced cytidine deaminase (AID) in complex with cacodylic acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-03-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9793 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.960, 179.070, 188.080 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 188.100 | 2.500 |
High resolution limit [Å] | 2.400 | 2.420 |
Rmerge | 0.109 | 1.354 |
Rpim | 0.577 | |
Number of reflections | 48976 | 53182 |
<I/σ(I)> | 11.4 | 1.5 |
Completeness [%] | 99.3 | 84.3 |
Redundancy | 11.9 | 5.6 |
CC(1/2) | 0.883 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 289 | 0.05 M sodium cacodylate at pH 5.5, 20 mM MgCl2, 10 mM CaCl2, 10 mM spermidine, 5% PEG3350 |