5SY7
Crystal Structure of the Heterodimeric NPAS3-ARNT Complex with HRE DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-08-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | P 43 |
Unit cell lengths | 64.831, 64.831, 249.102 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.842 - 4.200 |
R-factor | 0.2763 |
Rwork | 0.272 |
R-free | 0.36140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4zpk |
RMSD bond length | 0.004 |
RMSD bond angle | 0.731 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 4.270 |
High resolution limit [Å] | 4.200 | 11.360 | 4.200 |
Rmerge | 0.060 | 0.045 | 0.848 |
Number of reflections | 7195 | ||
<I/σ(I)> | 7.5 | ||
Completeness [%] | 94.6 | 93.2 | 72.3 |
Redundancy | 5.2 | 5.1 | 3.9 |
CC(1/2) | 0.982 | 0.893 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 289 | 100 mM NH4F, 9% PEG 3350 |