5N9W

Structure of adenylation domain THR1 involved in the biosynthesis of 4-chlorothreonine in Streptomyces SP.OH-5093, apo structure

Replaces:  5APL

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2.456 Å)

Cell axes177.63352.806108.861
Cell angles90.00105.8190.00
SpacegroupC 1 2 1
Resolution limits46.96 - 2.46
the highest resolution shell value2.522 - 2.456
R-factor0.2009
R-work0.19730
the highest resolution shell value0.275
R-free0.26990
the highest resolution shell value0.388
RMSD bond length0.009
RMSD bond angle1.205

Data Collection Statistics

Resolution limits50.00 - 2.46
the highest resolution shell value -
Number of reflections35853
Rmerge_l_obs0.140
the highest resolution shell value0.810
Completeness99.6
Redundancy6.7
the highest resolution shell value6.7
I/sigma(I)1

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, HANGING DROP6.5294

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*