5N38
S65DParkin and pUB complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-12-16 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9793 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 146.540, 146.540, 88.440 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.560 | 2.760 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.480 | |
Number of reflections | 17000 | |
<I/σ(I)> | 9.1 | 2.2 |
Completeness [%] | 96.4 | 88.4 |
Redundancy | 3.5 | 3.2 |
CC(1/2) | 0.640 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 100mM Tris pH 8.5, 200mM TMAO, PEG MME 2000 |