5JHG
Crystal structure of the complex between the human RhoA and the DH/PH domain of human ARHGEF11
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-05-20 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.541782 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 87.440, 118.589, 88.003 |
Unit cell angles | 90.00, 113.00, 90.00 |
Refinement procedure
Resolution | 31.130 - 2.500 |
R-factor | 0.22362 |
Rwork | 0.221 |
R-free | 0.27022 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.019 |
RMSD bond angle | 1.969 |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.540 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.073 | 0.530 |
Number of reflections | 56052 | |
<I/σ(I)> | 15.95 | |
Completeness [%] | 98.2 | 93.4 |
Redundancy | 4.1 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 293 | 2% v/v Tacsimate pH 5.0, 0.1M Sodium citrate tribasic dihydrate pH 5.6, 16% PEG 3350 |