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5J3X

Structure of c-CBL Y371F

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyCCD
Collection date2010-10-21
DetectorADSC QUANTUM 315
Wavelength(s)0.9763
Spacegroup nameC 2 2 21
Unit cell lengths147.842, 149.040, 344.118
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.371 - 2.822
R-factor0.2145
Rwork0.212
R-free0.25410
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2y1m
RMSD bond length0.002
RMSD bond angle0.544
Data reduction softwareXDS
Data scaling softwarexia2
Phasing softwarePHASER
Refinement softwarePHENIX (1.9_1692)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]105.0002.900
High resolution limit [Å]2.8202.820
Rmerge0.0750.489
Number of reflections91407
<I/σ(I)>9.72.4
Completeness [%]99.9100
Redundancy4.64.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.5281.15Equal volume protein at 10 mg/mL + well containing 3.0-3.1 M sodium formate 0.1 M Tris-HCl, pH 8.5 5 mM DTT

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