5FPB
Crystal structure of human KDM4D in complex with 2-1H-pyrazol-4-yloxy- 3H,4H-pyrido-3,4-d-pyrimidin-4-one
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-02-09 |
Detector | RIGAKU SATURN A200 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 71.180, 71.180, 150.788 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.150 - 1.910 |
R-factor | 0.16243 |
Rwork | 0.160 |
R-free | 0.20319 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | NONE |
RMSD bond length | 0.005 |
RMSD bond angle | 1.009 |
Data reduction software | XDS |
Data scaling software | SCALA |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.860 | 2.010 |
High resolution limit [Å] | 1.910 | 1.910 |
Rmerge | 0.060 | 0.420 |
Number of reflections | 30844 | |
<I/σ(I)> | 18.8 | 3.9 |
Completeness [%] | 99.6 | 99.8 |
Redundancy | 4.7 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.4 | 0.1M HEPES PH 7.4, 2.45M AMMONIUM SULPHATE |