Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-06-19 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97929 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 28.470, 72.166, 62.547 |
| Unit cell angles | 90.00, 101.77, 90.00 |
Refinement procedure
| Resolution | 46.690 - 1.780 |
| R-factor | 0.196 |
| Rwork | 0.194 |
| R-free | 0.24800 |
| Starting model (for MR) | 3TKZ AND 4XZ0 |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.690 | 1.820 |
| High resolution limit [Å] | 1.780 | 1.780 |
| Rmerge | 0.076 | 0.526 |
| Number of reflections | 23333 | |
| <I/σ(I)> | 11.2 | 1.4 |
| Completeness [%] | 98.5 | 95.9 |
| Redundancy | 3.9 | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 291 | 20% PEG-3350, 0.2 M ammonium formate |
