5CQD
Crystal Structure of the Cancer Genomic DNA Mutator APOBEC3B
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-06-21 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.440, 50.840, 70.150 |
Unit cell angles | 90.00, 100.83, 90.00 |
Refinement procedure
Resolution | 46.140 - 2.080 |
R-factor | 0.1897 |
Rwork | 0.188 |
R-free | 0.22680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3v4k |
RMSD bond length | 0.005 |
RMSD bond angle | 0.566 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2166: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.800 | 2.160 |
High resolution limit [Å] | 2.080 | 2.080 |
Rmerge | 0.446 | |
Number of reflections | 18464 | |
<I/σ(I)> | 12.4 | |
Completeness [%] | 86.0 | |
Redundancy | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG3350, MES-NaOH |