4YNQ
TREX1-dsDNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-02-13 |
Detector | RIGAKU SATURN 92 |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 83.142, 84.457, 103.000 |
Unit cell angles | 90.00, 102.15, 90.00 |
Refinement procedure
Resolution | 19.850 - 2.800 |
R-factor | 0.2198 |
Rwork | 0.218 |
R-free | 0.26630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2oa8 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.516 |
Data reduction software | d*TREK |
Data scaling software | d*TREK (9.9.9.1L) |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.850 | 19.850 | 2.900 |
High resolution limit [Å] | 2.800 | 5.980 | 2.800 |
Rmerge | 0.102 | 0.066 | 0.533 |
Total number of observations | 129430 | 13300 | 12505 |
Number of reflections | 25822 | ||
<I/σ(I)> | 5.4 | 14.6 | 1.2 |
Completeness [%] | 94.9 | 97.8 | 90.5 |
Redundancy | 3 | 3.5 | 2.56 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 298 | PEG 4000 |