4TOS
Crystal structure of Tankyrase 1 with 355
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-02-14 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9792372 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 48.195, 81.168, 114.155 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 31.000 - 1.802 |
| R-factor | 0.1823 |
| Rwork | 0.181 |
| R-free | 0.21070 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.013 |
| Phasing software | HKL-3000 |
| Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 31.000 |
| High resolution limit [Å] | 1.800 |
| Number of reflections | 41931 |
| <I/σ(I)> | 38.8 |
| Completeness [%] | 99.0 |
| Redundancy | 7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.1M Tris pH7.5, 0.2M sodium Acetate, 30% PEG4000 |
