4OVN
Voltage-gated Sodium Channel 1.5 (Nav1.5) C-terminal domain in complex with Calmodulin poised for activation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 31-ID |
Synchrotron site | APS |
Beamline | 31-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-04-07 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 106.128, 99.006, 109.281 |
Unit cell angles | 90.00, 106.11, 90.00 |
Refinement procedure
Resolution | 28.700 - 2.800 |
R-factor | 0.215 |
Rwork | 0.211 |
R-free | 0.28200 |
Structure solution method | MAD |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.900 | 2.850 |
High resolution limit [Å] | 2.798 | 2.800 |
Rmerge | 0.116 | 0.745 |
Total number of observations | 311500 | |
Number of reflections | 48516 | |
<I/σ(I)> | 11.5 | |
Completeness [%] | 90.3 | 58.3 |
Redundancy | 6.4 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 15% PEG 4K, 0.2 M MgSO4 and 10% glycerol |