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4LG8

Crystal structure of PRPF19 WD40 repeats

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU FR-E
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2013-03-04
DetectorRIGAKU RAXIS
Wavelength(s)1.5418
Spacegroup nameP 31 2 1
Unit cell lengths83.055, 83.055, 75.533
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution30.000 - 1.890
R-factor0.1581
Rwork0.156
R-free0.19680
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3ow8 2ymu 2co0
RMSD bond length0.016
RMSD bond angle1.458
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwareREFMAC
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]40.00040.0001.920
High resolution limit [Å]1.8905.1301.890
Rmerge0.0880.0520.986
Number of reflections24511
<I/σ(I)>10.6
Completeness [%]100.0100100
Redundancy10.39.69.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION29120% PEG-3350, 0.2 M disodium tartrate, vapor diffusion, temperature 291K

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