4LG8
Crystal structure of PRPF19 WD40 repeats
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-03-04 |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 83.055, 83.055, 75.533 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.000 | 40.000 | 1.920 |
High resolution limit [Å] | 1.890 | 5.130 | 1.890 |
Rmerge | 0.088 | 0.052 | 0.986 |
Number of reflections | 24511 | ||
<I/σ(I)> | 10.6 | ||
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 10.3 | 9.6 | 9.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 291 | 20% PEG-3350, 0.2 M disodium tartrate, vapor diffusion, temperature 291K |