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4EM9

Human PPAR gamma in complex with nonanoic acids

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsLNLS BEAMLINE W01B-MX2
Synchrotron siteLNLS
BeamlineW01B-MX2
Temperature [K]100
Detector technologyCCD
Collection date2008-02-07
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)1.46
Spacegroup nameC 1 2 1
Unit cell lengths92.731, 62.255, 118.649
Unit cell angles90.00, 101.94, 90.00
Refinement procedure
Resolution32.800 - 2.100
R-factor0.2065
Rwork0.205
R-free0.23510
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1zeo
RMSD bond length0.005
RMSD bond angle0.764
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]32.8002.155
High resolution limit [Å]2.1002.100
Number of reflections36859
Completeness [%]99.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.52910.1M tris-HCl, 0.9M sodium citrate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K

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